Regenerative NOx Removal

89% average NOx uptake over 14 days ofdiesel field operation

Krajete installed a mobile slipstream system on a diesel generator supplying off-grid drilling power. The pilot cooled exhaust from above 350 °C into the adsorption range, ran continuously for two weeks, and retained the captured nitrogen predominantly as nitrate for potential downstream recovery.

Client & context

Oil & gas drilling · Lower Austria · Diesel-generator exhaust · 14-day continuous pilot, February 2024

The problem, with a number

Generator exhaust entered the field problem above 350 °C, at a reported minimum NOx load of 350 ppm, varying with drilling duty and engine load.

What we measured

Testo 350 and 340 at inlet and outlet, twice daily, five-minute automated runs at one-second intervals across fourteen days.

What we did

Cooled and demisted a slipstream into a 280 L drum holding 130 kg of active adsorber, then dismantled the bed and analysed each layer.

What the campaign
had to handle

At least 350 ppm at the inlet

The generator exhaust entered the field problem at more than 350 °C and a reported minimum NOx load of 350 ppm.

The load never sits still

NOx concentration and gas flow varied with the drilling duty and the engine load behind it.

More than 300 °C to shed

The exhaust had to be cooled by over 300 °C before adsorption could be effective at all.

Remote sites punish complexity

A remote-site solution needed low parasitic power, simple operation, and a practical material-exchange route.

Stricter jurisdictions ahead

The operator sought more rigorous purification for work in jurisdictions such as the Netherlands, where low outlet concentrations may be required.

Destruction was not the goal

The customer wanted a regenerative pathway that keeps nitrogen as a recoverable nitrate stream, not only destructive conversion.

What does a 14-day field pilot actually involve?

Cool the gas, contact the bed, measure both ends, then take the adsorber apart and count what it kept.

Step 01

Take the slipstream

A fraction of one generator's exhaust, drawn without material backpressure on the engine.

Step 02

Cool and demist

Pipe extension, mechanical cooler and demister to 40 °C or below; condensate drained before the bed.

Step 03

Contact the bed

50–400 m³/h bottom-up through a 280 L drum holding 130 kg of active adsorber.

Step 04

Measure, then dismantle

Testo 350 and 340 twice daily for 14 days, then layer-by-layer TOC/TN and EDX analysis.

Instrumented at both ends. Verified inside the bed.

Fan demand averaged 220 W above 200 m³/h and peaked at 500 W. No electrical refrigeration was used during the pilot.

What the instruments recorded

At 400 m³/h a rising bed temperature cut uptake to 52% for a single day. Reducing flow to 300 and then 200 m³/h restored 70–83%; the run ended at 77% as the bed progressively loaded.

METRIC recorded basis
Inlet to outlet 401 to 43 ppm, average 89% average NOx uptake
Operating flow 50–400 m³/h Long-term table mean 221 m³/h
High-removal regime Above 95% uptake Held through 300 m³/h before heat and saturation effects
Gas treated At least 67,200 m³ 200 m³/h over 14 days; more than 100 tonnes
Active bed 200 L, 130 kg Inside a 280 L total drum volume
Nitrate loading 7.6 kg About 6 wt.% of dry adsorber, near 60% of saturation
Fan power 220 W average, 500 W peak Measured above 200 m³/h during the pilot

What the campaign looked like

NOx-Removal chart

Daily uptake against flow

Uptake tracked the slipstream flow: high through 300 m³/h, then falling as bed temperature and loading rose.

NOx-captured-as-Nitrate

Where the nitrogen ended up

The bed was separated layer by layer after the run and the loading profile quantified by total nitrogen analysis.

Field-Deployment

Real diesel exhaust.

Captured as nitrate.

Lower Austria, February 2024

89%

Average NOx uptake across the long-term measurement table

67,200 m³

Minimum gas volume treated over the 14-day run

7.6 kg

Nitrate retained on 130 kg of active adsorber

What the pilot was worth commercially

Risk taken out of the design

The campaign fixed field-specific removal, cooling, energy, capacity and mass-transfer data under real diesel exhaust.

Low parasitic demand

220 W average fan power above 200 m³/h, and 500 W at maximum load.

Design parameters identified

Roughly 500–1,000 h⁻¹ space velocity, about 35 cm mass-transfer zone, adsorption at or below 40 °C.

A regeneration pathway

Off-site thermal or heat and steam treatment, with heat preferred to preserve zeolite conditioning.

The trade-off made visible

Higher flow and rising bed temperature reduce capture; bed sizing and exchange logistics set cycle length.

No ROI is claimed

The source files document no realised ROI or operating-cost saving. The outcome at this stage is a validated pilot and a defined scale-up concept.

What was proposed next

After the campaign the operator asked for a solution covering two diesel containers with six engines, each at 1,500–2,000 m³/h cold dry off-gas. A validation phase of about three months is recommended before commitment. The source package documents a proposal, not an installed system.

Element Proposed specification Intended role
Core system 4 × 2,000 m³/h adsorbers, 8,000 m³/h total Most operation below 70% duty
Cooling Four custom air coolers to 40 °C Maintain the adsorption window
Fine polishing One 5,000 m³/h adsorber, target below 10 ppm Exceptional duty and stringent limits

What has to be proven before
commercial acceptance?

Measured evidence covers the 14-day campaign and post-run analysis. Sources: pilot report of 11 March 2024, offer 2024603 of 10 June 2024.

Next 01

Characterise the full stream

Cooled full-stream flow and NOx composition across the complete engine duty cycle.

Next 02

Scale the campaign

A 5–10× on-site adsorption run using roughly 1.4–3 m³, or 1–2 tonnes, of adsorber.

Next 03

Cycle the material

Repeated adsorption and regeneration, verifying nitrate recovery, material life, pressure drop and outlet targets.

YOUR LOAD CHANGES.

SO DOES YOUR NOx.

Discuss your exhaust profile, outlet target and regeneration strategy with a Krajete engineer. See regenerative NOx removal